健康食品中から検出されたタダラフィル類縁物質の構造解析

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タイトル別名
  • Structural Elucidation of a Tadalafil Analogue Found in a Dietary Supplement

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抄録

A tadalafil analogue was detected in a dietary supplement marketed for tonic effect, along with hydroxyhomosildenafil and aminotadalafil. The tadalafil analogue was isolated by preparative thin layer chromatography (TLC) and its structure was elucidated using high-performance liquid chromatography (HPLC), liquid chromatography electrospray ionization-mass spectrometry (LC-ESI-MS), Fourier transform-ion cyclotron resonance-mass spectrometry (FT-ICR-MS) and nuclear magnetic resonance (NMR) spectroscopy. The compound was determined to be methyl-1-(1,3-benzodioxol-5-yl)-2-(chloroacetyl)-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylate.

収録刊行物

  • 食品衛生学雑誌

    食品衛生学雑誌 49 (4), 311-315, 2008

    公益社団法人 日本食品衛生学会

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