畜水産食品中の残留オキシテトラサイクリンの分析法

DOI 日本農学文献記事索引 Web Site 被引用文献3件 参考文献19件

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タイトル別名
  • Analytical Method for Residual Oxytetracycline in Livestock and Marine Products.
  • チクスイサン ショクヒンチュウ ノ ザンリュウ オキシテトラサイクリン ノ ブ

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抄録

An analytical method for residual oxytetracycline (OTC) in livestock and marine products was evaluated. OTC was extracted from a sample with McIlvaine buffer (pH 4.0) containing 0.01mol/L EDTA-2 Na. The extract was washed with hexane, followed by a Sep-Pak Plus PS2 cartridge clean-up procedure. OTC was determined by HPLC. The results obtained by HPLC were well correlated with those of a microbioassay method. The average recovery at the tolerance limit levels established by the Food Sanitation Law of Japan was 90.4% and the determination limits were 0.02ppm (muscle, seafood, milk), 0.04ppm (liver, kidney, egg) and 0.002ppm (fat).

収録刊行物

  • 食品衛生学雑誌

    食品衛生学雑誌 38 (1), 12-15, 1997

    公益社団法人 日本食品衛生学会

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