Analytical Method for Residual Oxytetracycline in Livestock and Marine Products.
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- FUJITA Kazuhiro
- Japan Food Research Laboratories Nagoya Branch
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- ITO Kanako
- Japan Food Research Laboratories Nagoya Branch
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- ARAKI Emiko
- Japan Food Research Laboratories Head Office and Laboratory
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- TANNO Kenji
- Japan Food Research Laboratories Head Office and Laboratory
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- MURAYAMA Mitsunori
- National Institute of Health Sciences
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- SAITO Yukio
- National Institute of Health Sciences
Bibliographic Information
- Other Title
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- 畜水産食品中の残留オキシテトラサイクリンの分析法
- チクスイサン ショクヒンチュウ ノ ザンリュウ オキシテトラサイクリン ノ ブ
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Abstract
An analytical method for residual oxytetracycline (OTC) in livestock and marine products was evaluated. OTC was extracted from a sample with McIlvaine buffer (pH 4.0) containing 0.01mol/L EDTA-2 Na. The extract was washed with hexane, followed by a Sep-Pak Plus PS2 cartridge clean-up procedure. OTC was determined by HPLC. The results obtained by HPLC were well correlated with those of a microbioassay method. The average recovery at the tolerance limit levels established by the Food Sanitation Law of Japan was 90.4% and the determination limits were 0.02ppm (muscle, seafood, milk), 0.04ppm (liver, kidney, egg) and 0.002ppm (fat).
Journal
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- Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
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Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 38 (1), 12-15, 1997
Japanese Society for Food Hygiene and Safety
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Details 詳細情報について
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- CRID
- 1390001204223794560
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- NII Article ID
- 10009299818
- 10009711652
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- NII Book ID
- AN00117741
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- COI
- 1:CAS:528:DyaK2sXhvVKmtL0%3D
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- ISSN
- 18821006
- 00156426
- http://id.crossref.org/issn/00156426
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- NDL BIB ID
- 4151957
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- Text Lang
- ja
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- Data Source
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- JaLC
- IRDB
- NDL
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed