Analysis of Residual Synthetic Antibacterials in Meat and Poultry Meat by High Performance Liquid Chromatography
-
- HORII Shozo
- The Tokyo Metropolitan Research Laboratory of Public Health
-
- MIYAKAWA Hiroyuki
- The Tokyo Metropolitan Research Laboratory of Public Health
-
- IGUSA Kyoko
- The Tokyo Metropolitan Research Laboratory of Public Health
-
- ITOH Takeshi
- The Tokyo Metropolitan Research Laboratory of Public Health
Bibliographic Information
- Other Title
-
- 高速液体クロマトグラフィーによる食肉中の残留合成抗菌剤の分析
- コウソク エキタイ クロマトグラフィー ニ ヨル ショクニクチュウ ノ ザンリ
Search this article
Description
A simple and sensitive HPLC method is described for quantitative determination of some synthetic antibacterials in animal tissues. The compounds are divided into two groups, A and B. Tissue samples are extracted with acetonitrile and then group A is purified on a silicagel cartridge and group B by hexane partition; no other clean-up procedure is needed. Recoveries of the antibacterials spiked in animal tissue were 64-99%. The detection limits of quantitative determination by the proposed method were 0.01ppm for each antibacterial. The calibration curves for these compounds showed good linearity in the ranges of 0.5-50ng for carbadox, 1-100ng for thiamphenicol and furazolidone and 2-200ng for other drugs. Many chicken samples (total 121) which were purchased from a poultry processing plant in Tokyo were analyzed by the proposed method. Decoquinate was detected in two samples of chicken muscle at levels of 0.02 and 0.03ppm.
Journal
-
- Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
-
Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 35 (4), 352-356_1, 1994
Japanese Society for Food Hygiene and Safety
- Tweet
Keywords
Details 詳細情報について
-
- CRID
- 1390001204227295488
-
- NII Article ID
- 130003693254
-
- NII Book ID
- AN00117741
-
- ISSN
- 18821006
- 00156426
- http://id.crossref.org/issn/00156426
-
- NDL BIB ID
- 3897236
-
- Data Source
-
- JaLC
- IRDB
- NDL
- Crossref
- CiNii Articles
-
- Abstract License Flag
- Disallowed