高速液体クロマトグラフィーによる食肉中の残留合成抗菌剤の分析
書誌事項
- タイトル別名
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- Analysis of Residual Synthetic Antibacterials in Meat and Poultry Meat by High Performance Liquid Chromatography
- コウソク エキタイ クロマトグラフィー ニ ヨル ショクニクチュウ ノ ザンリ
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説明
A simple and sensitive HPLC method is described for quantitative determination of some synthetic antibacterials in animal tissues. The compounds are divided into two groups, A and B. Tissue samples are extracted with acetonitrile and then group A is purified on a silicagel cartridge and group B by hexane partition; no other clean-up procedure is needed. Recoveries of the antibacterials spiked in animal tissue were 64-99%. The detection limits of quantitative determination by the proposed method were 0.01ppm for each antibacterial. The calibration curves for these compounds showed good linearity in the ranges of 0.5-50ng for carbadox, 1-100ng for thiamphenicol and furazolidone and 2-200ng for other drugs. Many chicken samples (total 121) which were purchased from a poultry processing plant in Tokyo were analyzed by the proposed method. Decoquinate was detected in two samples of chicken muscle at levels of 0.02 and 0.03ppm.
収録刊行物
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- 食品衛生学雑誌
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食品衛生学雑誌 35 (4), 352-356_1, 1994
公益社団法人 日本食品衛生学会
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詳細情報 詳細情報について
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- CRID
- 1390001204227295488
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- NII論文ID
- 130003693254
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- NII書誌ID
- AN00117741
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- ISSN
- 18821006
- 00156426
- http://id.crossref.org/issn/00156426
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- NDL書誌ID
- 3897236
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- データソース種別
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- JaLC
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- NDL
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