Crystal Structure of 1-N-Methyl[2,2']spiro-acenaphthene-1'-one[3,2"]spiro-cyclohexane-1"-one-4-[p-methylphenyl]pyrrolidine

DOI Web Site 参考文献4件
  • PALANI K.
    Department of Crystallography and Biophysics, University of Madras
  • POORNACHANDRAN M.
    Department of Organic Chemistry, University of Madras, Guindy Campus
  • RAGHUNATHAN R.
    Department of Organic Chemistry, University of Madras, Guindy Campus
  • NETHAJI M.
    Department of Inorganic and Physical Chemistry, Indian Institute of Science
  • PONNUSWAMY M. N.
    Department of Crystallography and Biophysics, University of Madras

抄録

The title compound (C28H27NO2) crystallizes in monoclinic space group P21/c with a molecule in the asymmetric unit. The structure was solved by direct methods and refined by full-matrix least-squares procedures to final R = 0.0788 and wR = 0.2022 using 3083 reflections. The pyrrolidine and cyclohexane rings adopt envelope and chair conformations, respectively. The molecules are stabilized by C-H…O type intra and intermolecular interactions in addition to van der Waals forces.

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