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Synthesis of Brookite by Self-Hydrolysis:Effect of Synthetic Condition
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- Iwamoto Kazunori
- Kyushu University
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- Inada Miki
- Kyushu University
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- Enomoto Naoya
- Kyushu University
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- Hojo Junichi
- Kyushu University
Bibliographic Information
- Other Title
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- 自己加水分解によるブルッカイトの合成：合成条件の影響
Description
We have tried to synthesize brookite particles by self-hydrolysis of TiOCl2 with HCl addition. When 0.1M TiOCl2 with addition of 2M HCl was heated at 100°C for 24h by reflux method, brookite and rutole formed and the morphology was the agglutinated particle. on the other hand, when 0.075M TiOCl2 solution with addition of 2M HCl was heated at 100°C for 24h by using autoclave, particles of rutile and brookite formed and the morphology was the particle with a size of 4μm and the dispersed particle with a size of 100nm, respectively. The synthesized particles by using autoclave was separated to rutile and brookite because the brookite had high dispersibility.
Journal
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- Preprints of Annual Meeting of The Ceramic Society of Japan<br> Preprints of Fall Meeting of The Ceramic Society of Japan
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Preprints of Annual Meeting of The Ceramic Society of Japan<br> Preprints of Fall Meeting of The Ceramic Society of Japan 2010S (0), 1L23-1L23, 2010
The Ceramic Society of Japan
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Details 詳細情報について
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- CRID
- 1390001205619746816
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- NII Article ID
- 130006979036
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- Text Lang
- ja
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- Data Source
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- JaLC
- CiNii Articles
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- Abstract License Flag
- Disallowed