P15 Sonochemical Synthesis of Carbon Nanoparticles(Materials Synthesis, etc.)

DOI
  • ASO Ryota
    Department of Applied Chemistry, Faculty of Engineering, Kyushu University
  • MIYAJIMA Hohjun
    Department of Applied Chemistry, Faculty of Engineering, Kyushu University
  • UEHARA Masato
    Department of Applied Chemistry, Faculty of Engineering, Kyushu University
  • ENOMOTO Naoya
    Department of Applied Chemistry, Faculty of Engineering, Kyushu University
  • HOJO Junichi
    Department of Applied Chemistry, Faculty of Engineering, Kyushu University

Bibliographic Information

Other Title
  • P15 ソノケミカル反応によるカーボンナノ粒子の合成(物質創製、他)

Description

Sonochemical polymerization induced by applying ultrasound to benzene derivatives has been studied. Irradiating ultrasound to o-dichlorobenzene with solid particles such as zinc, its chloride, or nitrate produced various nanoparticles. In the case of using zinc nitrate, solid needle-like particles were obtained, when zinc metal and zinc nitrate were co-doped, hollow needle-like (tubular) particles were obtained. It is bound from the diffraction pattern that tubular particle has a polycrystalline structure, which could not be identified up to now. EDS analysis showed that the tubular particle contained Zinc element. When the particles were produced, Zinc element might be attracted inside or outside of the tubular particle. Various irradiation time and content of solid particles were tried, there might exist optimum parameter that increase a ratio of tubular particles respectively. In this research, the best parameter of the synthesis was; Irradiation time = 5 minutes Zinc: Zinc nitrate = 0.37wt%: 0.37wt% for o-dichlorobenzene.

Journal

Details 詳細情報について

  • CRID
    1390001206051343872
  • NII Article ID
    110009710233
  • DOI
    10.20577/pamjss.12.0_99
  • ISSN
    24241512
  • Text Lang
    ja
  • Data Source
    • JaLC
    • CiNii Articles
  • Abstract License Flag
    Disallowed

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