逆相高速液体クロマトグラフィーによる尿中有機溶剤代謝物の迅速定量
書誌事項
- タイトル別名
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- Rapid determination of organic solvent metabolites in urineby reversed phase HPLC.
- ギャクソウ コウソク エキタイ クロマトグラフィー ニ ヨル ニョウチュウ ユ
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We have developed an improved method for the determination of organic solvent metabolites(HAs), hippuric acid(HA), mandelic acid(MA), ο-methylhippuric acid(ο-MHA), m-methylhippuric acid (m-MHA), p-methylhippuric acid(p-MHA) and creatinine(CR), in urine by reversed phase HPLC. The separation was carried out with a stainless-steel column (4.0mm×200mm) packed with Wakosil II-5C18-100 and 8% 2-propano1/10mM phosphate buffer (pH2.4) containing 6mM 1-octanesulfonic acid sodium salt as a mobile phase (1.0ml/min). A UV monitor (210 nm) was used for monitoring. Reproducibility of this method was excellent. Calibration plots between 10 and 1000ng/injection were linear and passed through the origin of the coordinate system. This method was used for the determination of HAs in urine on volunteers.
収録刊行物
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- 分析化学
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分析化学 40 (12), 895-898, 1991
公益社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390282679028092544
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- NII論文ID
- 110002906215
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- NII書誌ID
- AN00222633
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- NDL書誌ID
- 3749498
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- ISSN
- 05251931
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
- NDL
- Crossref
- NDL-Digital
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可