Determination of Alanycarb in Agricultural Products by HPLC
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- ITO Masako
- The Tokyo Metropolitan Research Laboratory of Public Health
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- NAGAYAMA Toshihiro
- The Tokyo Metropolitan Research Laboratory of Public Health
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- KOBAYASHI Maki
- The Tokyo Metropolitan Research Laboratory of Public Health
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- HASHIMOTO Tsuneo
- The Tokyo Metropolitan Research Laboratory of Public Health
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- HANEISHI Nahoko
- The Tokyo Metropolitan Research Laboratory of Public Health
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- TAMURA Yasuhiro
- The Tokyo Metropolitan Research Laboratory of Public Health
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- TOMOMATSU Toshio
- The Tokyo Metropolitan Research Laboratory of Public Health
Bibliographic Information
- Other Title
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- HPLCによる農産物中アラニカルブの分析法
Description
A simplified determination procedure for alanycarb in agricultural products by high performance liquid chromatography with a UV detector was developed.<br>The homogenate of agricultural products was extracted with acetone. The crude extract was partitioned between 10% sodium chloride solution and ethyl acetate, and the ethyl acetate layer was evaporated to dryness. The residue was dissolved in n-hexane, and the solution was cleaned up on a Bond Elute® extraction cartridge PSA, then analyzed by liquid chromatography. Alanycarb was detected by measuring the absorbance at 230nm.<br>Recoveries at the 0. 1ppm level were more than 70% from agricultural products except brown rice. Detection limits for the products were 0.01ppm in samples.
Journal
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- Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
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Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 39 (3), 218-224_1, 1998
Japanese Society for Food Hygiene and Safety
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Details 詳細情報について
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- CRID
- 1390282679203342592
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- NII Article ID
- 130003693505
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- ISSN
- 18821006
- 00156426
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- Data Source
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- JaLC
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed