Determination of Alanycarb in Agricultural Products by HPLC

Bibliographic Information

Other Title
  • HPLCによる農産物中アラニカルブの分析法

Description

A simplified determination procedure for alanycarb in agricultural products by high performance liquid chromatography with a UV detector was developed.<br>The homogenate of agricultural products was extracted with acetone. The crude extract was partitioned between 10% sodium chloride solution and ethyl acetate, and the ethyl acetate layer was evaporated to dryness. The residue was dissolved in n-hexane, and the solution was cleaned up on a Bond Elute® extraction cartridge PSA, then analyzed by liquid chromatography. Alanycarb was detected by measuring the absorbance at 230nm.<br>Recoveries at the 0. 1ppm level were more than 70% from agricultural products except brown rice. Detection limits for the products were 0.01ppm in samples.

Journal

Details 詳細情報について

  • CRID
    1390282679203342592
  • NII Article ID
    130003693505
  • DOI
    10.3358/shokueishi.39.3_218
  • ISSN
    18821006
    00156426
  • Data Source
    • JaLC
    • Crossref
    • CiNii Articles
  • Abstract License Flag
    Disallowed

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