コメ中のフモニシンB1, B2, B3の液体クロマトグラフィーによる定量
書誌事項
- タイトル別名
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- Liquid chromatographic determination of fumonisins B1, B2, and B3 in rice
- 公開日
- 2007
- 資源種別
- journal article
- DOI
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- 10.2520/myco.57.95
- 公開者
- 日本マイコトキシン学会
この論文をさがす
説明
Rice is susceptible to the fungus Gibberella fujikuroi, the anamorph of which is taxonomically near to Fusarium verticillioides, a major fumonisin producer, so that the potential risk of fumonisin contamination in rice is significant. However, most works on fumonisins have examined corn or wheat and there have not been any practical methods developed for the analysis of fumonisins in rice. This paper describes the development of liquid chromatographic determination methods with an efficient extraction procedure for fumonisins (fumonisin B1, B2, and B3) in rice, using artificially molded rice contaminated with fumonisins. Applied with submergence extraction, stable and sufficient recovery was achieved for various rice samples in spike and recovery tests. The determination was done by liquid chromatography using fluorescence detection (HPLC-FL) with precolumn derivatization, or using tandem mass spectrometry (LC-MS/MS). The limit of detection achieved by LC-MS/MS was ten times lower than that by HPLC-FL for fumonisin B1.
収録刊行物
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- マイコトキシン
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マイコトキシン 57 (2), 95-104, 2007
日本マイコトキシン学会
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詳細情報 詳細情報について
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- CRID
- 1390282679760872832
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- NII論文ID
- 10021920199
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- NII書誌ID
- AN00334513
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- COI
- 1:CAS:528:DC%2BD1cXntVOktrc%3D
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- ISSN
- 18810128
- 02851466
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- 本文言語コード
- en
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- 資料種別
- journal article
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- データソース種別
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- JaLC
- IRDB
- Crossref
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可
